In the laboratory, Wang Manshan watched as the two high-frequency induction furnaces were ready, and the two operators next to him were actively debugging!
There are two backup power supplies next to it just in case.
"Old Wang, Yang Bi said that, believe in his own feelings!"
"It's nothing if you fail, don't have any psychological burden!"
Wang Manshan and Zheng pointed at the key point, "Uh, understand!"
"Don't worry!"
Finally, I added, "You talk about the key points, I'm afraid I won't remember it!"
Li Lei didn't mind either and told the meticulous operation process!
"I understand, I understand!"
Wang Manshan said he remembered it and said, "Nine hundred, not too high or too low!"
"Nine hundred, nine hundred!"
As Wang Manshan muttered, the operator received instructions to start the experiment.
First, put the treated quartz powder into the crucible of the high-frequency induction furnace, and then add 6 parts of reducing agent.
There is a piece of bronze in the high-frequency induction furnace on the right.
Everything was ready, Wang Manshan squatted down and waved to Li Lei.
Instantly, the power is turned on.
High-frequency AC power begins to enter the copper tube, and then an induced current appears in the objects inside.
Under the operator's control, this induced current quickly enters the copper coil.
The high-frequency induction furnace started to work, and the harsh sound accompanied by heat made Wang Manshan very uncomfortable, but he still looked forward and carefully.
Mr. Peng and Mr. Chen both watched with intent eyes. Mr. Ye came to the front and explained to the two.
"This is a high-frequency induction furnace, simply by using the heat it releases, to melt itself..."
"It acts directly inside the object."
“This way can achieve rapid heating.”
"However, safety is a major hidden danger. Safety assessment must be carried out after each use, and demagnetization must be carried out before each use!"
"Also, the strength of the power supply must be guaranteed..."
Mr. Ye said aside, Mr. Peng and his two listened seriously.
Not only that, others are also focused.
Yang Xiaotao also added on the side, and Han Sanfeng waved to make someone record carefully.
These are the processes given by the system.
Because the system gives technology with all the preparations, this is very different from reality.
But what Mr. Ye said is something that can be used in reality.
Or it could be improved many years later, and perhaps better high-frequency induction furnaces will be developed, but now, they can only use these.
“It’s been changed!”
Li Hongfeng looked at the bronze lights coming out of the stove on the right and began to melt. Everyone hurriedly looked at it.
This is the suggestion made by Mr. Ye.
The melting points of some known special metals are used as standards to determine the gear position of the high-frequency induction furnace.
The melting point of bronze is about 800 degrees, which is just right for use.
They have done several experiments in the early stage and can basically determine the frequency required.
This experiment is also for the sake of foolproof, otherwise it would be a high-frequency induction furnace.
However, what makes Yang Xiaotao a pity is that he did not find the metal with a melting point of 900 degrees.
Even so, Mr. Peng and Mr. Chen, who were familiar with the situation, nodded with relief.
There are always more ways than difficulties.
Obviously, Jiubi has used his brains in this regard.
So, after the next rise to 900 degrees, it depends on Wang Manshan’s golden eyes!
"Team leader Wang, it's 800 yuan, pay attention!"
Li Lei shouted and went straight to the high-frequency induction furnace to get started by himself.
Wang Manshan nodded slightly after hearing this!
At this time, Wang Manshan looked at him without blinking, and even if the sweat flowed down his forehead, he would not dare to touch it with his hands, for fear of missing the time!
At the same time, his hand slowly raised and then gently pressed down.
Every time he waved down, Li Lei on the side would increase the frequency a little.
As time goes by, the frequency of Wang Manshan's hand waving began to slow down.
The people outside were anxious to see it, but they didn't dare to say anything more, just staring at Wang Manshan's every move inside!
Gradually, it got dark outside.
The lights in the laboratory did not light up.
Just as everyone was waiting anxiously, they suddenly saw Wang Manshan reaching out and pressing down quickly.
Li Lei was shocked, and his hand moved, and the button turned a little more.
The next second, Wang Manshan sat on the ground, wiping the sweat on his face and laughing.
Li Lei quickly recorded the frequency of the current high-frequency induction furnace, and then made people start to flip the boiler inside.
At this step, they need to constantly reverse the transfer of it fully reacts with the reducing agent.
At this time, Wang Manshan turned around and waved his hand to the person watching outside, showing a sure smile.
In an instant, people around us hugged each other, followed by cheers, which lasted for a long time!
Mr. Peng and Mr. Chen were also infected. Seeing everyone happy, they applauded involuntarily.
Slap
Applause was given to Wang Manshan, Li Lei and others inside, and also to people outside.
After the applause stopped, Yang Xiaotao quickly reminded everyone, "Please pay attention, we are not over yet."
"Director Zhu, you must be prepared next."
Zhu Ziqing walked out and shouted loudly, "Please, please don't worry, Yang's army, we are ready long ago."
Not far away, people from the Chemistry Institute immediately walked out.
Seeing that everyone was ready, Yang Xiaotao stopped talking and watched the changes in the induction furnace seriously!
According to the process requirements, after continuous flipping at a high temperature of 900 degrees and sufficient reaction, crude silicon can be obtained!
It lasts for more than an hour before the high-frequency induction furnace ends the reaction.
After waiting for more than an hour, Li Lei took out the cooling boiler according to the process requirements and quickly cooled it down.
Yang Xiaotao quickly moved forward, looking at the gray crystal inside, and a look of relief appeared on his face.
This form has shown that at least half of the success!
The next operation falls into the category of chemical reactions!
Yang Xiaotao looked at Zhu Ziqing, "Let's see you next!"
Zhu Ziquan nodded, "I understand!"
After saying that, Zhu Ziqing took people to wear protective clothing, gloves, and goggles, and her whole body was wrapped tightly!
Although it was cold outside, the temperature in the laboratory was not low. If you were in such a whole body, you would probably sweat all over.
Zhu Ziqing looked at the people behind him, nodded, and then led the group into the laboratory.
This chapter is not over, please click on the next page to continue reading! Check out the instruments and equipment in it, and after checking, start to arrange tasks!
According to the process requirements, everyone put the obtained crude silicon into the reactor again.
Then another 6 parts of the reactant were injected...
Mr. Peng and Mr. Wang were watching, and Yang Xiaotao chatted with Mr. Ye for a while before he came to the front.
"President Peng, Chief, the next reaction will take a lot of time. Why don't we go to have a meal first?"
Mr. Peng shook his head, "I'm not hungry, you can go and eat when you are hungry!"
Yang Xiaotao looked at Mr. Chen again, and Mr. Chen shook his head.
Now they have no intention of having a meal!
These two people don’t eat them anymore, so no one else dares to eat them.
So everyone continued to wait outside.
This wait was straight to dawn the next day.
When it was dawn outside, Yang Xiaotao heard something behind him. When he looked back, Mr. Peng had already moved his hands and feet and walked towards him!
Not many people were present, after all, they still needed work.
Besides, Old Ye is old and can’t hold on, so he lets him go back to the office to rest!
The rest are Yang Xiaotao, Li Hongfeng, President Peng, Lao Chen, and the guards in charge of security around them.
Seeing that Mr. Chen was still resting aside, Yang Xiaotao said to the guards on duty not far away, "Let the kitchen arrange more food!"
The guard nodded and left gently.
Mr. Peng came to Yang Xiaotao, looked at the busy scene inside, and then asked, "How long has it been?"
Yang Xiaotao looked at his watch, "It's been eight hours!"
"How is the situation?"
Yang Xiaotao rubbed his face and nodded, "It's going well!"
After all, this is also the first live experiment.
There is only one process operation diagram in the process given by the system, and the specific situation must be based on actual conditions.
Mr. Peng nodded, but his eyes were staring at the lab in the room.
In this environment, persisting for such a long time not only requires physical support, but also a firm will!
Yang Xiaotao took out the cigarette box and found that there was only one left in it. He then put it back in his pocket.
"I didn't expect it would take so long!"
"The reaction is so complicated!"
Mr. Peng stood with his hands behind his back, "This is what we said. The knowledge on paper is shallow. You must practice it yourself!"
"If you don't do it, you will never know where the gap is!"
Yang Xiaotao nodded slightly.
Still not prepared enough!
When the reaction is first started, the amount of reaction reagents required is too small, resulting in incomplete reaction.
When the second step was to collect the gas, I found that the color inside was not right, and there was still a lot of quartz powder in the reactor.
Obviously, the experimental response is not thorough, which will affect the experimental results.
So everyone looked for the reason, but later they found that it was not the fault of the process requirements, but the insufficient purity of the reaction reagent and insufficient addition amount.
After reconciling, the experiment was conducted again and finally obtained silicon tetrachloride gas.
Then the operation is carried out now, hydrogen gas is heated into the reactor at high temperature to fully react, producing high-purity pure silicon and hydrogen chloride gas.
If you want to implement these simple steps, you can find them step by step!
The experiment was able to proceed smoothly, and this was all due to Zhu Ziqing, the professor of chemistry!
“Is this going to end?”
Mr. Peng watched the people inside come together, as if observing something.
Yang Xiaotao came to his senses and hurriedly looked at him. He saw Zhu Ziqing suddenly raised his head and waved to Yang Xiaotao.
"Success?"
Li Hongfeng also ran over when he heard the movement and was very curious.
Mr. Chen also stood up not far away.
"I don't know, let's talk about it."
Yang Xiaotao stared inside and soon saw Zhu Ziqing walking out holding a reaction dish.
The four of them were busy waiting.
"Yangbu, see if this is high-purity silicon."
Zhu Ziqing walked up to Yang Xiaotao, his voice feeling exhausted.
The researchers behind them walked out and helped each other take off their protective suits, revealing their sweaty figures.
At this moment, the four people were looking at the small reaction dish.
A small pile of blue-gray crystals.
It looks a bit like crystal, but very small.
Even when the sun shines in, there is a metallic color.
Yang Xiaotao carefully took the reaction dish and his breathing became lighter, as if he was afraid that he would blow away with force.
"That's it, silicon?"
Mr. Peng asked in a low voice.
Mr. Chen rubbed his eyes and looked carefully, trying to see what was different from what he imagined.
Li Hongfeng didn't know what this was, but all three of them looked at it, and he came over to look at it.
Yang Xiaotao compared the information introduced in the ultra-pure silicon production process, and then nodded vigorously, "Yes, this is silicon!"
“A thing that can bring about change in the world.”
After hearing this, Mr. Peng and the other two looked at each other.
If they hadn't seen it with their own eyes, this thing was extracted from the stone, which would have been incredible.